摘要本课题采用相对低温的水热合成方法,制备出ZnO/BC杂化纤文。采用紫外-可见吸收光谱、傅里叶红外光谱、X射线衍射、扫描电子显微镜和热重分析表征对杂化纤文进行微观表征。由XRD图谱可以看出,杂化纤文上所负载的ZnO呈现吹冰方纤锌矿晶型;SEM表征ZnO尺寸大小在200nm,并均匀地分散在纤文表面,在此基础上采用傅里叶红外光谱分析材料的结构;紫外-可见吸收光谱用来进一步分析材料的光学吸收性能;上述表征结果显示,在细菌纤文素模板上以成功的制备出和纯纳米ZnO相比直径较小、长径比均一,微观形貌更为突出的纳米ZnO。
关键词 半导体材料 纤文素 纳米ZnO 模板效应 4943
毕业设计说明书(论文)外文摘要
Title :A preliminary study of ZnO visible light photocatalytic prepared by bacterial cellulose as template.
Abstract
Nano-sized zinc oxide was synthesized and deposited onto bacterial cellulose(BC) fibers using the hydrothermal process at relatively low temperature. The prepared materials were characterized using several techniques including scanning electron microscopy, UV-vis absortion spectroscopy, Fourier transform infrared spectroscopy(FTIR), X-ray diffraction and thermogravimetric analysis. X-ray diffraction studies of the ZnO-coated fiber indicate formation of the hexagonal crystal phase which was satisfactory crystallized on the fiber surface. The electron micrographs show formation of zinc oxide nanoparticles about 200nm in size which have been homogeneously dispersed on the BC fibers . The structure of the prepared materials were characterized by Fourier transform infrared spectroscopy(FTIR).The UV-vis absorption of ZnO was carried out for further analysis of the optical absorption property of the material.The results of characterization reveals that we successfully prepared a ZnO nanorod used BC as template with homogeneous aspect ratio and splendid morphology compare to the pure ZnO nanorod.
Keywords Nano-sized zinc oxide, Bacterial cellulose, ZnO nanorod, Template